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Synthesis of inherently chiral calixarenes via direct mercuration of the partial cone conformation

. 2016 Feb 07 ; 52 (11) : 2366-9.

Status PubMed-not-MEDLINE Language English Country England, Great Britain Media print

Document type Journal Article, Research Support, Non-U.S. Gov't

Direct mercuration of calix[4]arene immobilized in the partial cone conformation led to the meta-substituted isomer which was subsequently subjected to Pd-catalysed coupling (C-H activation) with the neighbouring aromatic subunit. Regioselective mercuration thus enabled access to a novel type of inherently chiral calixarenes with a highly distorted cavity potentially applicable to the design of new chiral receptors.

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Upper rim-bridged calixarenes

. 2024 Jul 19 ; 14 (32) : 23303-23321. [epub] 20240724

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