• Je něco špatně v tomto záznamu ?

Microwave-assisted synthesis of new substituted anilides of quinaldic acid

P. Bobal, J. Sujan, J. Otevrel, A. Imramovsky, Z. Padelkova, J. Jampilek,

. 2012 ; 17 (2) : 1292-1306. [pub] 20120131

Jazyk angličtina Země Švýcarsko

Typ dokumentu časopisecké články, práce podpořená grantem

Perzistentní odkaz   https://www.medvik.cz/link/bmc12024066

In this study a one step method for the preparation of substituted anilides of quinoline-2-carboxylic acid was developed. This efficient innovative approach is based on the direct reaction of an acid or ester with substituted anilines using microwave irradiation. The optimized method was used for the synthesis of a series of eighteen substituted quinoline-2-carboxanilides. The molecular structure of N-(4-bromophenyl)quinoline-2-carboxamide as a model compound was determined by single-crystal X-ray diffraction. It crystallizes in the monoclinic space group with four molecules within the unit cell and the total structure of the compound can be described as "a slightly screwed boat".

Citace poskytuje Crossref.org

000      
00000naa a2200000 a 4500
001      
bmc12024066
003      
CZ-PrNML
005      
20170410103934.0
007      
ta
008      
120815s2012 sz f 000 0#eng||
009      
AR
024    7_
$a 10.3390/molecules17021292 $2 doi
035    __
$a (PubMed)22293847
040    __
$a ABA008 $b cze $d ABA008 $e AACR2
041    0_
$a eng
044    __
$a sz
100    1_
$a Bobal, Pavel $u Department of Chemical Drugs, University of Veterinary and Pharmaceutical Sciences, Palackeho 1/3, 612 42 Brno, Czech Republic. bobalp@vfu.cz
245    10
$a Microwave-assisted synthesis of new substituted anilides of quinaldic acid / $c P. Bobal, J. Sujan, J. Otevrel, A. Imramovsky, Z. Padelkova, J. Jampilek,
520    9_
$a In this study a one step method for the preparation of substituted anilides of quinoline-2-carboxylic acid was developed. This efficient innovative approach is based on the direct reaction of an acid or ester with substituted anilines using microwave irradiation. The optimized method was used for the synthesis of a series of eighteen substituted quinoline-2-carboxanilides. The molecular structure of N-(4-bromophenyl)quinoline-2-carboxamide as a model compound was determined by single-crystal X-ray diffraction. It crystallizes in the monoclinic space group with four molecules within the unit cell and the total structure of the compound can be described as "a slightly screwed boat".
650    _2
$a anilidy $x chemická syntéza $x chemie $7 D000813
650    _2
$a krystalografie rentgenová $7 D018360
650    _2
$a hmotnostní spektrometrie $7 D013058
650    _2
$a mikrovlny $7 D008872
650    _2
$a chinoliny $x chemie $7 D011804
655    _2
$a časopisecké články $7 D016428
655    _2
$a práce podpořená grantem $7 D013485
700    1_
$a Sujan, Josef
700    1_
$a Otevrel, Jan
700    1_
$a Imramovsky, Ales
700    1_
$a Padelkova, Zdenka
700    1_
$a Jampilek, Josef
773    0_
$w MED00180394 $t Molecules (Basel, Switzerland) $x 1420-3049 $g Roč. 17, č. 2 (2012), s. 1292-1306
856    41
$u https://pubmed.ncbi.nlm.nih.gov/22293847 $y Pubmed
910    __
$a ABA008 $b sig $c sign $y m $z 0
990    __
$a 20120815 $b ABA008
991    __
$a 20170410104232 $b ABA008
999    __
$a ok $b bmc $g 946214 $s 781394
BAS    __
$a 3
BAS    __
$a PreBMC
BMC    __
$a 2012 $b 17 $c 2 $d 1292-1306 $e 20120131 $i 1420-3049 $m Molecules $n Molecules $x MED00180394
LZP    __
$a Pubmed-20120815/12/02

Najít záznam

Citační ukazatele

    Možnosti archivace