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A practical approach for synthesis of biodiesel via non-edible seeds oils using trimetallic based montmorillonite nano-catalyst

M. Munir, M. Ahmad, M. Mubashir, S. Asif, A. Waseem, A. Mukhtar, S. Saqib, H. Siti Halimatul Munawaroh, MK. Lam, K. Shiong Khoo, A. Bokhari, P. Loke Show

. 2021 ; 328 (-) : 124859. [pub] 20210217

Jazyk angličtina Země Velká Británie

Typ dokumentu časopisecké články

Perzistentní odkaz   https://www.medvik.cz/link/bmc21011382

The potential of new trimetallic (Ce, Cu, La) loaded montmorillonite clay catalyst for synthesizing biodiesel using novel non-edible Celastrus paniculatus Willd seed oil via two-step transesterification reaction has been reported along with catalyst characterization. Transesterification reaction was optimized and maximum biodiesel yield of 89.42% achieved under optimal operating reaction states like; 1:12 oil to methanol ratio, 3.5% of catalyst amount, 120 °C of reaction temperature for 3 h. The predicted and experimental biodiesel yields under these reaction conditions were 89.42 and 89.40%, which showing less than 0.05% variation. Additionally, optimum biodiesel yield can be predicted by drawing 3D surface plots and 2D contour plots using MINITAB 17 software. For the characterization of the obtained biodiesel, analysis including the GC/MS, FT-IR, 1H NMR and 13C NMR were applied. The fuel properties of obtained biodiesel agrees well with the different European Union (EU-14214), China (GB/T 20828), and American (ASTM-951, 6751) standards.

Citace poskytuje Crossref.org

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$a Munir, Mamoona $u Department of Plant Sciences, Quaid-i-Azam University, 45320 Islamabad, Pakistan
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$a A practical approach for synthesis of biodiesel via non-edible seeds oils using trimetallic based montmorillonite nano-catalyst / $c M. Munir, M. Ahmad, M. Mubashir, S. Asif, A. Waseem, A. Mukhtar, S. Saqib, H. Siti Halimatul Munawaroh, MK. Lam, K. Shiong Khoo, A. Bokhari, P. Loke Show
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$a The potential of new trimetallic (Ce, Cu, La) loaded montmorillonite clay catalyst for synthesizing biodiesel using novel non-edible Celastrus paniculatus Willd seed oil via two-step transesterification reaction has been reported along with catalyst characterization. Transesterification reaction was optimized and maximum biodiesel yield of 89.42% achieved under optimal operating reaction states like; 1:12 oil to methanol ratio, 3.5% of catalyst amount, 120 °C of reaction temperature for 3 h. The predicted and experimental biodiesel yields under these reaction conditions were 89.42 and 89.40%, which showing less than 0.05% variation. Additionally, optimum biodiesel yield can be predicted by drawing 3D surface plots and 2D contour plots using MINITAB 17 software. For the characterization of the obtained biodiesel, analysis including the GC/MS, FT-IR, 1H NMR and 13C NMR were applied. The fuel properties of obtained biodiesel agrees well with the different European Union (EU-14214), China (GB/T 20828), and American (ASTM-951, 6751) standards.
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$a Ahmad, Mushtaq $u Department of Plant Sciences, Quaid-i-Azam University, 45320 Islamabad, Pakistan
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$a Mubashir, Muhammad $u Department of Petroleum Engineering, School of Engineering, Asia Pacific University of Technology and Innovation, 57000 Kuala Lumpur, Malaysia
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$a Asif, Saira $u Faculty of Sciences, Department of Botany, PMAS Arid Agriculture University, Rawalpindi, Punjab 46300, Pakistan; Sustainable Process Integration Laboratory, SPIL, NETME Centre, Faculty of Mechanical Engineering, Brno University of Technology, VUT Brno, Technická 2896/2, 616 00 Brno, Czech Republic
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$a Waseem, Amir $u Department of Chemistry, Quaid-i-Azam University, 45320 Islamabad, Pakistan
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$a Mukhtar, Ahmad $u Department of Chemical Engineering, NFC Institute of Engineering and Fertilizer Research Faisalabad, 38000, Pakistan
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$a Saqib, Sidra $u Chemical Engineering Department, COMSATS University Islamabad (CUI), Lahore Campus, Lahore, Punjab 54000, Pakistan
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$a Siti Halimatul Munawaroh, Heli $u Study Program of Chemistry, Department of Chemistry Education, Universitas Pendidikan Indonesia, Jl. Dr. Setiabudhi 229, Bandung 40154, Indonesia
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$a Lam, Man Kee $u Department of Chemical Engineering, HICoE-Centre for Biofuel and Biochemical Research, Institute of Self-Sustainable Building, Universiti Teknologi PETRONAS, 32610 Seri Iskandar, Perak Darul Ridzuan, Malaysia
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$a Shiong Khoo, Kuan $u Department of Chemical and Environmental Engineering, Faculty of Science and Engineering, University of Nottingham Malaysia, Jalan Broga, Semenyih 43500, Selangor Darul Ehsan, Malaysia
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$a Bokhari, Awais $u Sustainable Process Integration Laboratory, SPIL, NETME Centre, Faculty of Mechanical Engineering, Brno University of Technology, VUT Brno, Technická 2896/2, 616 00 Brno, Czech Republic; Chemical Engineering Department, COMSATS University Islamabad (CUI), Lahore Campus, Lahore, Punjab 54000, Pakistan
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$a Loke Show, Pau $u Department of Chemical and Environmental Engineering, Faculty of Science and Engineering, University of Nottingham Malaysia, Jalan Broga, Semenyih 43500, Selangor Darul Ehsan, Malaysia. Electronic address: PauLoke.Show@nottingham.edu.my
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