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CALIBRATION OF A TABLETOP CONFOCAL MICROBEAM X-RAY FLUORESCENCE SPECTROMETER FOR A QUANTITATIVE DEPTH PROFILES EVALUATION
R. Prokeš, T. Trojek,
Jazyk angličtina Země Velká Británie
Typ dokumentu hodnotící studie, časopisecké články
PubMed
31845991
DOI
10.1093/rpd/ncz216
Knihovny.cz E-zdroje
- MeSH
- algoritmy MeSH
- fluorescence * MeSH
- kalibrace MeSH
- lidé MeSH
- rentgenové záření MeSH
- spektrometrie rentgenová emisní přístrojové vybavení metody normy MeSH
- Check Tag
- lidé MeSH
- Publikační typ
- časopisecké články MeSH
- hodnotící studie MeSH
Confocal micro-beam X-ray fluorescence analysis (confocal micro-XRF) is a non-destructive analytical tool for investigation of sample composition that enables acquiring three-dimensionally resolved information. This work describes a calibration procedure of a laboratory confocal micro-XRF setup, which leads to determination of its characteristic parameters. The calibration is performed using a tabletop confocal micro-XRF spectrometer designed recently at the Czech Technical University in Prague. The calibration procedure performed within this work comprises the essential steps of the setup characterization: excitation spectrum calculation, experimental determination of energy-dependent confocal volume size and integral sensitivity and calculation of the spectrometer sensitivity function. The results of the setup calibration will be used for development of a procedure enabling quantitative evaluation of the measured depth profiles.
Citace poskytuje Crossref.org
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