We report on the growth of metal- and metal-oxide based nanoparticles (NPs) in heated polyol solutions. For this purpose, NPs are produced by the sputtering of a silver, gold, or a copper target to produce either silver, gold, or copper oxide NPs in pentaerythritol ethoxylate (PEEL) which has been annealed up to 200 °C. The objective of the annealing step is the fine modulation of their size. Thus, the evolution of the NP size and shape after thermal annealing is explained according to collision/coalescence kinetics and the affinity between the metal-/metal-oxide and PEEL molecule. Moreover, highlights of few phenomena arising from the annealing step are described such as (i) the reduction of copper oxide into copper by the polyol process and (ii) the effective formation of carbon dots after annealing at 200 °C.

Chimie des Interactions Plasma Surface University of Mons Place du Parc 20 7000 Mons Belgium

Department of Chemical Physics and Optics Faculty of Mathematics and Physics Charles University Ke Karlovu 5 121 16 Praha 2 Czech Republic

Department of Condensed Matter Physics Faculty of Mathematics and Physics Charles University Ke Karlovu 5 121 16 Praha 2 Czech Republic

Department of Physics of Materials Faculty of Mathematics and Physics Charles University Ke Karlovu 5 121 16 Praha 2 Czech Republic

Institute of Physics of the Czech Academy of Sciences Cukrovarnická 10 112 162 00 Prague 6 Czech Republic

Laboratory for Chemistry of Novel Materials University of Mons Place du Parc 20 Mons 7000 Belgium

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