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Use of residual dipolar couplings in conformational analysis of meta-disubstituted calix[4]arenes

. 2014 Jul 21 ; 50 (57) : 7590-2.

Status PubMed-not-MEDLINE Language English Country England, Great Britain Media print

Document type Journal Article

Persistent link   https://www.medvik.cz/link/pmid24820209

Dimercuration of tetrapropoxy calix[4]arene followed by a reaction with isoamyl nitrite afforded dinitroso regioisomers with unique substitution patterns. The unusual conformational behaviour of these inherently chiral systems was revealed by the combination of dynamic NMR and residual dipolar coupling (RDC) techniques.

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