Influence of surface pre-treatment with mechanical polishing, chemical, electrochemical and ion sputter etching on the surface properties, corrosion resistance and MG-63 cell colonization of commercially pure titanium
Language English Country Netherlands Media print-electronic
Document type Journal Article
PubMed
32600690
DOI
10.1016/j.msec.2020.111065
PII: S0928-4931(20)30368-4
Knihovny.cz E-resources
- Keywords
- Corrosion resistance, MG-63 cell behaviour, Surface characterization, Surface pre-treatment, Titanium,
- MeSH
- Cell Line MeSH
- Electrochemical Techniques MeSH
- Corrosion MeSH
- Humans MeSH
- Oxides chemistry MeSH
- Surface Properties MeSH
- Materials Testing MeSH
- Titanium chemistry MeSH
- Hardness MeSH
- Check Tag
- Humans MeSH
- Publication type
- Journal Article MeSH
- Names of Substances
- Oxides MeSH
- Titanium MeSH
The impact of four pre-treatment techniques on the surface morphology and chemistry, residual stress, mechanical properties, corrosion resistance in a physiological saline solution and cell colonization of commercially pure titanium is examined in detail. Mechanical polishing, electrochemical etching, chemical etching in Kroll's reagent, and ion sputter etching with argon ions were applied. Surface morphologies reflect the nature of surface layer removal. Significant roughening of the surface and a characteristic microtopology become apparent as a result of the sensitivity of chemical and ion sputter etching to the grain orientation. The hardness in the near surface region was controlled by the amount of residual stress. Etching of the stressed surface layer led to a reduction in residual stress and surface hardness. A compact passivation layer composed of TiO, TiO2 and Ti2O3 native oxides imparted high corrosion resistance to the surface after mechanical polishing, chemical and electrochemical etching. The ion sputter etched surface showed substantially reduced corrosion resistance, where the corrosion process was controlled by electron transfer. The specific topology affected the adhesion of the cell to the surface rather than the cell area coverage. The cell area coverage increased with the corrosion stability of the surface.
References provided by Crossref.org
