Detail
Article
Online article
FT
Medvik - BMC
  • Something wrong with this record ?

Determination of N-methylcarbamates in foods

I Borkovcová, E. Janoušková, I. Řehůřková

. 2004 ; 12 (4) : 220-223.

Language English Country Czech Republic

Persistent link   https://www.medvik.cz/link/bmc05005948

The multiresidue method using multisolvent extraction, SPE cleanup of the extract, HPLC with the use of OPA post-column reaction and fluorescence detection for the determination of N-methylcarbamate pesticides in food products was used. A matrix solid phase dispersion method of the isolation and extraction of carbamates was alternatively applied. In the introductory study 44 items of the food basket for the Czech Republic were analysed. In the major part of the studied samples, the considerable part of which was culinary treated, the concentration of the target carbamates was below the limit of the used detection method. In the concentration range of 10–100 μg/kg in the analysed samples of the studied analytes, aldicarb and its metabolites, e.g. methomyl and methiocarb were being found most frequently.

Bibliography, etc.

Lit. 12

000      
00000naa a2200000 a 4500
001      
bmc05005948
003      
CZ-PrNML
005      
20140110142927.0
008      
050603s2004 xr u eng||
009      
AR
040    __
$a ABA008 $b cze $c ABA008 $d ABA008 $e AACR2
041    0_
$a eng
044    __
$a xr
100    1_
$a Borkovcová, I. $4 aut
245    10
$a Determination of N-methylcarbamates in foods / $c I Borkovcová, E. Janoušková, I. Řehůřková
314    __
$a The National Institute of Public Health in Prague, Division for the Hygiene of Food Chains, Brno, CZ
504    __
$a Lit. 12
520    9_
$a The multiresidue method using multisolvent extraction, SPE cleanup of the extract, HPLC with the use of OPA post-column reaction and fluorescence detection for the determination of N-methylcarbamate pesticides in food products was used. A matrix solid phase dispersion method of the isolation and extraction of carbamates was alternatively applied. In the introductory study 44 items of the food basket for the Czech Republic were analysed. In the major part of the studied samples, the considerable part of which was culinary treated, the concentration of the target carbamates was below the limit of the used detection method. In the concentration range of 10–100 μg/kg in the analysed samples of the studied analytes, aldicarb and its metabolites, e.g. methomyl and methiocarb were being found most frequently.
650    _2
$a HERBICIDY KARBAMÁTOVÉ $x analýza $x izolace a purifikace $x škodlivé účinky
650    _2
$a agrochemikálie $x analýza $x škodlivé účinky $7 D016573
650    _2
$a kontaminace potravin $7 D005506
650    _2
$a vysokoúčinná kapalinová chromatografie $x metody $7 D002851
650    _2
$a chemické techniky analytické $x metody $7 D002623
650    _2
$a kontrola potravin $7 D005513
650    _2
$a techniky in vitro $7 D066298
700    1_
$a Janoušková, Eva $4 aut $7 xx0101706
700    1_
$a Řehůřková, I. $4 aut
700    1_
$a Ruprich, Jiří, $d 1954- $4 aut $7 ola2002110019
773    0_
$w MED00001083 $t Central European journal of public health $g Roč. 12/48, č. 4 (2004), s. 220-223 $x 1210-7778
856    41
$u https://cejph.szu.cz/pdfs/cjp/2004/04/13.pdf $y plný text volně přístupný
910    __
$a ABA008 $b B 1829 $c 562 $y 0 $z 0
990    __
$a 20050614 $b ABA008
991    __
$a 20140110143630 $b ABA008
BAS    __
$a 3
BMC    __
$a 2004 $b 12 $c 4 $d 220-223 $i 1210-7778 $m Central European Journal of Public Health $x MED00001083
LZP    __
$b přidání abstraktu
Back

Find record

Citation metrics

Archiving options