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N-acylated bacteriohopanehexol-mannosamides from the thermophilic bacterium Alicyclobacillus acidoterrestris
T. Rezanka, L. Siristova, K. Melzoch, K. Sigler,
Language English Country Germany
Document type Journal Article, Research Support, Non-U.S. Gov't
NLK
ProQuest Central
from 1997-01-01 to 2017-12-31
Health & Medicine (ProQuest)
from 1997-01-01 to 2017-12-31
Public Health Database (ProQuest)
from 1997-01-01 to 2017-12-31
- MeSH
- Acylation MeSH
- Alicyclobacillus chemistry growth & development MeSH
- Amides analysis chemistry isolation & purification MeSH
- Spectrometry, Mass, Electrospray Ionization MeSH
- Magnetic Resonance Spectroscopy MeSH
- Mannose analysis chemistry MeSH
- Gas Chromatography-Mass Spectrometry MeSH
- Tandem Mass Spectrometry MeSH
- Temperature MeSH
- Triterpenes analysis chemistry isolation & purification MeSH
- Chromatography, High Pressure Liquid MeSH
- Publication type
- Journal Article MeSH
- Research Support, Non-U.S. Gov't MeSH
Identification of molecular species of various N-acylated bacteriohopanehexol-mannosamides from the thermophilic bacterium Alicyclobacillus acidoterrestris by semipreparative HPLC and by RP-HPLC with ESI is described. We used triple-quadrupole type mass spectrometer, (1)H and (13)C NMR for analyzing this complex lipid. CD spectra of two compounds (model compound--7-deoxy-D: -glycero-D: -allo-heptitol obtained by stereospecific synthesis, and an isolated derivative of hopane) were also measured and the absolute configuration of both compounds was determined. On the basis of all the above methods, we identified the full structure of a new class of bacteriohopanes, represented by various N-acylated bacteriohopanehexol-mannosamides.
References provided by Crossref.org
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