Sewage and water networks are crucial infrastructures of modern urban society. The uninterrupted functionality of these networks is paramount, necessitating regular maintenance and rehabilitation. In densely populated urban areas, trenchless methods, particularly those employing cured-in-place pipe technology, have emerged as the most cost-efficient approach for network rehabilitation. Common diagnostic methods for assessing pipe conditions, whether original or retrofitted with-cured-in-place pipes, typically include camera examination or laser scans, and are limited in material characterization. This study introduces three innovative methods for characterizing critical aspects of pipe conditions. The impact-echo method, ground-penetrating radar, and impedance spectroscopy address the challenges posed by polymer liners and offer enhanced accuracy in defect detection. These methods enable the characterization of delamination, identification of caverns behind cured-in-place pipes, and evaluation of overall pipe health. A machine learning algorithm using deep learning on images acquired from impact-echo signals using continuous wavelet transformation is presented to characterize defects. The aim is to compare traditional machine learning and deep learning methods to characterize selected pipe defects. The measurement conducted with ground-penetrating radar is depicted, employing a heuristic algorithm to estimate caverns behind the tested polymer composites. This study also presents results obtained through impedance spectroscopy, employed to characterize the delamination of polymer liners caused by uneven curing. A comparative analysis of these methods is conducted, assessing the accuracy by comparing the known positions of defects with their predicted characteristics based on laboratory measurements.

• Keywords
• cured-in-place pipes, machine learning, non-destructive testing, pipe defects, polymers, retrofitting,
• Publication type
• Journal Article MeSH

Measurement of thermal resistance of polymer sheets and fibrous layers is important in various applications including those within the engineering, ergonomics, clothing design and personal protective equipment fields. Standard methods for measurement of thermal resistance of plain materials are generally time consuming, expensive and often require the sample to be cut. Moreover, the temperature difference between the surfaces of both plates surrounding the sample must be known, as well as the sample thickness. This article describes a new measuring device named the Thermoscope. The Thermoscope is not limited by the aforementioned requirements and is able to evaluate the thermal resistance of polymer sheets and textiles by touching the sample on one surface alone. Simultaneously, the other surface is kept in thermal contact with the supporting base. The accuracy of this device was compared with the Alambeta thermal insulation tester. Effects of various base materials on measurement precision were also studied.

• Keywords
• fibrous layer, non-destructive testing, single plate, thermal resistance,
• MeSH
• Polymers MeSH
• Thermal Conductivity MeSH
• Materials Testing instrumentation   methods   MeSH
• Textiles MeSH
• Publication type
• Journal Article MeSH
• Names of Substances
• Polymers MeSH

Radiation-shielding concrete has been analyzed by several methods of destructive and non-destructive testing (NDT). Concretes made of crushed basalt, magnetite, serpentinite, and two different types of cement (Portland cement CEM I and slag cement CEM III/A) were studied. In this study, we analyzed concrete columns with a height of 1200 mm and a cross-section of 200 × 200 mm2. The top and bottom of the column were analyzed using data from compressive strength, dynamic modulus of elasticity, water penetration, and diffusion coefficients derived from the electrical resistivity test. This article presents the properties of fresh concrete and concrete after two years of setting. It was determined how the different ratios of basalt, magnetite, and serpentinite affect the individual measured parameters. Furthermore, correlation relations between individual resulting values were analyzed. It was observed that compressive strength generally does not correlate with other results. The diffusion coefficient correlated well with density and water penetration. Little or no correlation was observed in the diffusion coefficient with compressive strength and modulus of elasticity. The results of the study make it possible to refine the testing of heavy concretes in terms of electrical resistivity, and point to the possible use of NDT methods. The results also show which composition of heavy concrete is better in terms of effective diffusivity.

• Keywords
• NDT, Portland cement, diffusion, magnetite aggregate, radiation-shielding concrete, self-compacting concrete, serpentine aggregate, slag cement,
• Publication type
• Journal Article MeSH

This paper deals with the description, measurement, and use of electromagnetic properties of ferromagnetic fibres used as dispersed fibre reinforcement in composite mixtures. Firstly, the fibres' magnetic properties are shown, and a method of measuring the hysteresis loop of fibres is proposed. The results from the measurements are presented and a discussion of the influence of measured parameters on the fibres' orientation in a magnetic field is performed. Furthermore, methods of non-destructive estimation, of their amount and orientation in the composite specimens, are discussed. The main experimental goal of this paper is to show the relationship between this non-destructive method's results and the destructive flexural strength measurements. The method is sensitive enough to provide information related to fibre reinforcement.

• Keywords
• UHPFRC, cementitious composite, concrete, fibre, magnetic field, orientation, quality factor,
• Publication type
• Journal Article MeSH

Poly(ɛ-caprolactone) (PCL) is a biocompatible, biodegradable, and highly mechanically resilient FDA-approved material (for specific biomedical applications, e.g. as drug delivery devices, in sutures, or as an adhesion barrier), rendering it a promising candidate to serve bone tissue engineering. However, in vivo monitoring of PCL-based implants, as well as biodegradable implants in general, and their degradation profiles pose a significant challenge, hindering further development in the tissue engineering field and subsequent clinical adoption. To address this, photo-cross-linkable mechanically resilient PCL networks are developed and functionalized with a radiopaque monomer, 5-acrylamido-2,4,6-triiodoisophthalic acid (AATIPA), to enable non-destructive in vivo monitoring of PCL-based implants. The covalent incorporation of AATIPA into the crosslinked PCL networks does not significantly affect their crosslinking kinetics, mechanical properties, or thermal properties, but it increases their hydrolysis rate and radiopacity. Complex and porous 3D designs of radiopaque PCL networks can be effectively monitored in vivo. This work paves the way toward non-invasive monitoring of in vivo degradation profiles and early detection of potential implant malfunctions.

• Keywords
• computed tomography contrast agent, implant, light‐based 3D printing, light‐based crosslinking, photo‐crosslinkable polymers, polyester, thiol‐ene step growth polymerization,
• MeSH
• Biocompatible Materials chemistry   MeSH
• Mice MeSH
• Polyesters * chemistry   MeSH
• Porosity MeSH
• Materials Testing MeSH
• Tissue Engineering methods   MeSH
• Tissue Scaffolds * chemistry   MeSH
• Absorbable Implants MeSH
• Animals MeSH
• Check Tag
• Mice MeSH
• Animals MeSH
• Publication type
• Journal Article MeSH
• Names of Substances
• Biocompatible Materials MeSH
• polycaprolactone MeSH Browser
• Polyesters * MeSH

Additive manufacturing has many positives, but its incorporation into functional parts production is restricted by the presence of defects. Eddy current testing provides solutions for their identification; however, some methodology and measurement standards for AM (additive manufacturing) products are still missing. The main purpose of the experiment described within this article was to check the ability of eddy current testing to identify AM stainless steel parts and to examine the data obtained by eddy currents variation under the influence of various types of designed artificial defects. Experimental samples were designed and prepared with SLM (selective laser melting) technology. Artificial defects, included in the samples, were detected using the eddy current testing device, taking the important circumstances of this non-destructive method into account. The presented research shows significant potential for eddy current testing to identify defects in AM products, with a resolution of various types and sizes of defects. The obtained data output shows the importance of choosing the right measurement regime, excitation frequency and secondary parameters setup. Besides the eddy current testing conditions, defect properties also play a significant role, such as their shape, size, if they are filled with unmolten powder or if they reach the surface.

• Keywords
• additive manufacturing, artificial defects, eddy current, non-destructive testing, selective laser melting, stainless steel,
• Publication type
• Journal Article MeSH

Alkali-activated systems (AAS) represent an ecologically and economically sustainable inorganic binder as an alternative to ordinary Portland cement (OPC). One of the main benefits of AAS is their durability in aggressive environments, which can be equal or even better than that of OPC. In this paper, the influence of the type of alkaline activator in alkali-activated blast furnace slag (AAS) in terms of resistance to sulfur dioxide corrosion was investigated. The durability testing process was based on the CSN EN ISO 3231 standard and simultaneously compared with mortar samples prepared by using Blastfurnace cement CEM III/A 32.5R. The degradation progress was evaluated by employing several different methods such as observing the compressive strength development, weight change evaluation, non-destructive testing methods like ultrasound or impact echo technique, or visual phenolphthalein technique. Subsequently, fundamental characterization of samples by the XRD method was performed during the degradation test. The obtained results indicate that none of the testing methods used could be prioritized over others to determine the resistance of AAS against the action of sulfur dioxide. For this reason, the durability testing of AAS remains an issue, and the development of specific standards considering the behavior of AAS seems necessary.

• Keywords
• alkaline activation, blast furnace slag, corrosion resistance, degradation characterization, non-destructive testing, sulfur dioxide,
• Publication type
• Journal Article MeSH

Determination of chemosensitivity/chemoresistance is becoming increasingly important for individualization of breast cancer chemotherapy. We developed a simple non-destructive test of cellular activity (NTCA) for assessment of the cytopathic effect of antitumour drugs in vitro. Contrary to routinely used methods (e.g. MTT), besides the comparative evaluation of metabolic activity using pH (given by the medium colour), the NTCA enables the simultaneous assessment of proliferation and morphology of cultured cells (phase-contrast microscopy) at any time during the incubation with cytostatics. Moreover, the regenerative potential of the cells can be examined by cell recovery and growth after drug removal. We provide evidence for the relevance of NTCA in chemosensitivity testing of primary breast cancer cells and breast cancer cell lines for cisplatin, gemcitabine and tamoxifen. NTCA represents a simple addition to the chemosensitivity assessment and could also serve for rapid screening of new antitumour strategies.

• MeSH
• Cell Line MeSH
• Cell Growth Processes drug effects   MeSH
• Cisplatin administration & dosage   MeSH
• Deoxycytidine analogs & derivatives   pharmacology   MeSH
• Gemcitabine MeSH
• Humans MeSH
• Mammary Glands, Human cytology   drug effects   MeSH
• Cell Line, Tumor MeSH
• Breast Neoplasms drug therapy   metabolism   pathology   MeSH
• Antineoplastic Agents pharmacology   MeSH
• Antineoplastic Combined Chemotherapy Protocols pharmacology   MeSH
• Receptors, Estrogen biosynthesis   MeSH
• Reproducibility of Results MeSH
• Drug Screening Assays, Antitumor methods   MeSH
• Tamoxifen administration & dosage   MeSH
• Tetrazolium Salts MeSH
• Thiazoles MeSH
• Check Tag
• Humans MeSH
• Female MeSH
• Publication type
• Journal Article MeSH
• Research Support, Non-U.S. Gov't MeSH
• Names of Substances
• Cisplatin MeSH
• Deoxycytidine MeSH
• Gemcitabine MeSH
• Antineoplastic Agents MeSH
• Receptors, Estrogen MeSH
• Tamoxifen MeSH
• Tetrazolium Salts MeSH
• Thiazoles MeSH
• thiazolyl blue MeSH Browser

The detection of defects in aluminium alloys using eddy current testing (ECT) can be restricted by higher electrical conductivity. Considering the occurrence of discontinuities during the selective laser melting (SLM) process, checking the ability of the ECT method for the mentioned purpose could bring simple and fast material identification. The research described here is focused on the application of three ECT probes with different frequency ranges (0.3-100 kHz overall) for the identification of artificial defects in SLM aluminium alloy AlSi10Mg. Standard penetration depth for the mentioned frequency range and identification abilities of used probes expressed through lift-off diagrams precede the main part of the research. Experimental specimens were designed in four groups to check the signal sensitivity to variations in the size and depth of cavities. The signal behavior was evaluated according to notch-type and hole-type artificial defects' presence on the surface of the material and spherical cavities in subsurface layers, filled and unfilled by unmolten powder. The maximal penetration depth of the identified defect, the smallest detectable notch-type and hole-type artificial defect, the main characteristics of signal curves based on defect properties and circumstances for distinguishing between the application of measurement regime were stated. These conclusions represent baselines for the creation of ECT methodology for the defectoscopy of evaluated material.

• Keywords
• AlSi10Mg, additive manufacturing, eddy current, non-destructive testing, selective laser melting,
• Publication type
• Journal Article MeSH

The potential nondestructive diagnostics of solid objects is discussed in this article. The whole process is accomplished by consecutive steps involving software analysis of the vibration power spectrum (eventually acoustic emissions) created during the normal operation of the diagnosed device or under unexpected situations. Another option is to create an artificial pulse, which can help us to determine the actual state of the diagnosed device. The main idea of this method is based on the analysis of the current power spectrum density of the received signal and its postprocessing in the Matlab environment with a following sample comparison in the Statistica software environment. The last step, which is comparison of samples, is the most important, because it is possible to determine the status of the examined object at a given time. Nowadays samples are compared only visually, but this method can't produce good results. Further the presented filter can choose relevant data from a huge group of data, which originate from applying FFT (Fast Fourier Transform). On the other hand, using this approach they can be subjected to analysis with the assistance of a neural network. If correct and high-quality starting data are provided to the initial network, we are able to analyze other samples and state in which condition a certain object is. The success rate of this approximation, based on our testing of the solution, is now 85.7%. With further improvement of the filter, it could be even greater. Finally it is possible to detect defective conditions or upcoming limiting states of examined objects/materials by using only one device which contains HW and SW parts. This kind of detection can provide significant financial savings in certain cases (such as continuous casting of iron where it could save hundreds of thousands of USD).

• Keywords
• FFT, MatLab, Statistica, defect, power spectrum,
• MeSH
• Acoustics MeSH
• Online Systems MeSH
• Signal Processing, Computer-Assisted MeSH
• Software MeSH
• Spectrum Analysis methods   MeSH
• Vibration * MeSH
• Publication type
• Journal Article MeSH
• Research Support, Non-U.S. Gov't MeSH