The fatigue behavior of a filled non-crystallizing elastomer was investigated on axisymmetric dumbbell specimens. By plotting relevant Wöhler curves, a power law behavior was found. In addition, temperature increases due to heat build-up were monitored. In order to distinguish between initiation and crack growth regimes, hysteresis curves, secant and dynamic moduli, dissipated and stored energies, and normalized minimum and maximum forces were analyzed. Even though indications related to material damaging were observed, a clear trend to recognize the initiation was not evident. Further details were revealed by considering a fracture mechanics. The analysis of the fracture surfaces evidenced the presence of three regions, associated to initiation, fatigue striation, and catastrophic failure. Additional fatigue tests were performed with samples in which a radial notch was introduced. This resulted in a reduction in lifetime by four orders of magnitude; nevertheless, the fracture surfaces revealed similar failure mechanisms. A fracture mechanics approach, which considered the effect of temperature, was adopted to calculate the critical defect size for fatigue, which was found to be approximately 9 μm. This value was then compared with the particle size distribution obtained through X-ray microcomputed tomography (μ-CT) of undamaged samples and it was found that the majority of the initial defects were indeed smaller than the calculated one. Finally, the evaluation of J-integral for both unnotched and notched dumbbells enabled the assessment of a geometry-independent correlation with fatigue life.

• Klíčová slova
• J-integral, X-ray microtomography, defect size, fatigue, filled rubber, fracture mechanics, temperature,
• Publikační typ
• časopisecké články MeSH

OBJECTIVES: The adhesion tests utilized in dentistry are unable to separate the effects of adhesive composition, substrate properties, joint geometry and type of loading on the measured bond strength. This makes it difficult for the clinician to identify the most suitable adhesive for a given procedure and for the adhesive manufacturer to optimize its composition. Thus, an adhesion test protocol based on the fracture mechanics has been proposed to generate data for which separation of the effect of composition from that of the joint geometry on the shear (τ(a)) and tensile (σ(a)) bond strengths was possible for five commercial dental adhesives. METHODS: Planar 40×5×5 mm(3) sections of bovine femur were used as model adherends. The adhesive thickness (h) was varied from 15 to 500 μm. Commercial adhesives with fracture toughness (K(IC)) ranging from 0.3 to 1.6 MPa m(1/2) were used. Double lap joint (DLJ) and modified compact tension (MCT) specimens were conditioned for 24 h in 37 °C distilled water, then dried in a vacuum oven at 37 °C for 24 h prior to testing. The thickness dependence of σ(a) and τ(a) was measured at constant strain rate and analyzed using the interface corner stress intensity factor model. RESULTS: Both τ(a) and σ(a) increased with increasing adhesive thickness, exhibiting a maximum bond strength at the optimum thickness (h(opt)). For h

• MeSH
• femur metabolismus   MeSH
• mechanické jevy * MeSH
• pevnost v tahu MeSH
• skot MeSH
• testování materiálů metody   MeSH
• zubní cementy chemie   metabolismus   MeSH
• zvířata MeSH
• Check Tag
• skot MeSH
• zvířata MeSH
• Publikační typ
• časopisecké články MeSH
• práce podpořená grantem MeSH
• Názvy látek
• zubní cementy MeSH

Diamond-reinforced metal matrix composites (DMMC) prepared by cold spray are emerging materials simultaneously featuring outstanding thermal conductivity and wear resistance. In our paper, their mechanical and fatigue properties relevant to perspective engineering applications were investigated using miniature bending specimens. Two different diamond mass concentrations (20 and 50%) embedded in two metal matrices (Al-lighter than diamond, Cu-heavier than diamond) were compared with the respective cold-sprayed pure metals, as well as bulk Al and Cu references. The pure Al, Cu coatings showed properties typical for cold spray deposits, i.e., decreased elastic moduli (50 GPa for Al, 80 GPa for Cu), limited ductility (< 1 × 10-3) and low fracture toughness (3.8 MPa·m0.5 for Al, 5.6 MPa·m0.5 for Cu) when compared to the bulks. Significantly improved properties (strain at fracture, ultimate strength, fatigue crack growth resistance, fracture toughness) were then observed for the produced DMMC. The improvement can be explained by a combination of two factors: changes in the properties of the metallic matrix triggered by the reinforcement particles peening effect and stress redistribution due to the particles presence.

• Klíčová slova
• cold spray, processing diamond metal matrix composites, mechanical properties, properties, properties, fatigue, properties, fracture,
• Publikační typ
• časopisecké články MeSH
• přehledy MeSH

The study was aimed at the clinical and biomechanical analyses of the sliding hip screw breakage with the use of finite element method. We have identified two patients with the sliding screw breakage. In the first patient, the biomechanical analysis revealed the reduced stress values σHMH not exceeding the yield limit or strength limit of the implant. The yield limit was exceeded in second one. Clinical and biomechanical analyses have demonstrated that adherence to technical requirements of the appropriate osteosynthesis implementation is the principal condition of timely healing since it prevents the material failure.

• Klíčová slova
• Sliding hip screw, fatigue failure, finite element method, non-union,
• MeSH
• biomechanika MeSH
• fraktury kyčle diagnostické zobrazování   patofyziologie   MeSH
• kostní šrouby * MeSH
• lidé středního věku MeSH
• lidé MeSH
• mechanický stres * MeSH
• selhání protézy * MeSH
• senioři nad 80 let MeSH
• teoretické modely MeSH
• testování materiálů MeSH
• Check Tag
• lidé středního věku MeSH
• lidé MeSH
• mužské pohlaví MeSH
• senioři nad 80 let MeSH
• ženské pohlaví MeSH
• Publikační typ
• časopisecké články MeSH
• kazuistiky MeSH

Fatigue tests were performed on the AZ91 cast alloy to identify the mechanisms of the fatigue crack initiation. In different fatigue regions, different mechanisms were observed. In the low and high cycle fatigue regions, slip markings formation accompanied with Mg17Al12 particles cracking were observed. Slip markings act as the fatigue crack initiation sites. The size and number of slip markings decreased with decreased stress amplitude applied. When slip markings formation was suppressed due to low stress amplitude, particle cracking became more important and the cracks continued to grow through the particle/solid solution interface. The change of the fatigue crack initiation mechanisms led the S-N curve to shift to the higher number of cycles to the fracture, demonstrated by its stepwise character. A lower fatigue limit of 60 MPa was determined at 20 kHz for 2 × 109 cycles compared to the 80 MPa determined at 60 Hz for 1 × 107 cycles.

• Klíčová slova
• Mg, fatigue mechanism, focused ion beam (FIB), microstructure, scanning electron microscopy (SEM),
• Publikační typ
• časopisecké články MeSH

The magnesium AZ31 alloy was swaged with rotary pressure with the aim of redefining the microstructure and improving mechanical and fatigue properties. The rotary swaging process and subsequent ageing improved the yield stress in tension and compression. In the present study, the investigation was focused on fatigue behaviour. The samples were cycled in a symmetric regime with a frequency of 35 Hz. A dependence of the stress amplitude on the number of cycles up to the fracture was estimated. The microstructure of the samples and fracture surfaces was analysed with a scanning electron microscope. The fatigue process was influenced by the pronounced texture formed in the swaging process. The fatigue properties of the swaged samples improved substantially-the endurance limit based on 107 cycles was approximately 120 MPa-compared to those of the cast alloy. The analysis of the fracture surfaces showed a transcrystalline fatigue fracture.

• Klíčová slova
• fatigue life, fractography, magnesium alloy AZ31, non-basal slip, rotary swaging, twinning,
• Publikační typ
• časopisecké články MeSH

A fitting method capable of describing the fatigue crack growth rate (FCGR) data in all stages of crack propagation by a simple Forman-style analytical formula was developed. To demonstrate its robustness, this method was used to quantify the fracture behavior of RF-plasma-sprayed W, Mo, W-Mo composite, and four selected Ni-based tungsten heavy alloys (WHA). The fitted FCGR parameters categorized the studied materials into two distinct sets. W, Mo, and W-Mo composite deposits made from inherently brittle refractory metals that contained a range of defects inherent to plasma spray process represented the first class. This class was characterized by low fracture toughness and a relatively wide range of fatigue crack growth thresholds. The second class of materials was represented by WHA. Here, the deposit defects were suppressed by liquid state diffusion that formed a typical WHA structure consisting of a Ni-rich matrix and large spherical W reinforcement particles. The WHA generally showed higher fatigue crack growth thresholds, but differed in fracture toughness values based on the W particle concentrations. The obtained fracture mechanical data represent a reference dataset of plasma-sprayed refractory materials, and their classification into groups clearly demonstrates the capabilities of the developed method to capture a wide range of different types of FCGR behavior.

• Klíčová slova
• RF plasma spray, analytical model, fatigue crack growth, refractory materials,
• Publikační typ
• časopisecké články MeSH

OBJECTIVE: To evaluate the influence of different types of modifications with resin on fatigue resistance and failure behavior of CAD-CAM resin nano ceramic (RNC) restorations for maxillary first premolars. METHODS: Sixty standardized resin composite root dies received CAD-CAM RNC endocrowns (n=30) and crowns (n=30) (Lava Ultimate, 3M Espe). Restorations were divided into six groups: full anatomic endocrowns (group A) and crowns (group D), buccal resin veneered endocrowns (group B) and crowns (group E) and buccal resin veneered endocrowns (group C) and crowns (group F) with a central groove resin filling. A nano-hybrid resin composite was used to veneer the restorations (Filtek Supreme, 3M Espe). All specimens were first submitted to thermo-mechanical cyclic loading (1.7Hz, 49N, 600000 cycles, 1500 thermo-cycles) and then submitted to cyclic isometric stepwise loading (5Hz) until completion of 105000 cycles or failure after 5000 cycles at 200N, followed by 20000 cycles at 400N, 600N, 800N, 1000N and 1200N. In case of fracture, fragments were analyzed using SEM and modes of failure were determined. Results were statistically analyzed by Kaplan-Meier life survival analysis and log rank test (p=0.05). RESULTS: The differences in survival between groups were not statistically significant, except between groups D and F (p=0.039). Endocrowns fractured predominantly with a mesio-distal wedge-opening fracture (82%). Partial cusp fractures were observed above all in crowns (70%). Analysis of the fractured specimens revealed that the origin of the fracture was mainly at the occlusal contact points of the stepwise loading. SIGNIFICANCE: Veneering of CAD-CAM RNC restorations has no influence on their fatigue resistance except when monolithic crowns are modified on their occlusal central groove.

• Klíčová slova
• CAD/CAM, Endocrown, Endodontically treated teeth, Fatigue, Fractography, Lava Ultimate, Veenering,
• MeSH
• analýza zatížení zubů MeSH
• design s pomocí počítače * MeSH
• složené pryskyřice MeSH
• zubní korunky * MeSH
• zubní porcelán * MeSH
• Publikační typ
• časopisecké články MeSH
• Názvy látek
• složené pryskyřice MeSH
• zubní porcelán * MeSH

The fatigue properties of thermo-mechanically treated and machined aluminum alloy 7475-T7351 have been studied. The applied advanced machining strategy induced intensive plastic deformation on the machined surface under defined cutting conditions. Therefore, a detailed study of 3D surface topography was performed. Advanced characterization of the material structure and electron back scattered diffraction mapping of selected chemical phases were performed, as well as energy dispersive X-ray analysis of the surface. Advanced mechanical properties of the material were investigated in situ with a scanning electron microscope that was equipped with a unique tensile fixture. The fatigue results confirmed an evident dispersion of the data, but the mechanism of crack nucleation was established. Fracture surface analysis showed that the cracks nucleated at the brittle secondary particles dispersed in the material matrix. The surface topography of samples that had been machined in wide range of cutting/deformation conditions by milling has not proved to be a decisive factor in terms of the fatigue behavior. The incoherent interface and decohesion between the alumina matrix and the brittle secondary phases proved to significantly affect the ultimate strength of the material. Tool engagement also affected the fatigue resistance of the material.

• Klíčová slova
• crack nucleation, fatigue, plastic deformation, surface topography,
• Publikační typ
• časopisecké články MeSH

STATEMENT OF PROBLEM: Fatigue failure of implant components is a common clinical problem. Plasma nitriding, an in situ surface-strengthening method, may improve fatigue properties of dental implants. PURPOSE: The purpose of this in vitro study was to evaluate the effect of plasma nitriding on the fatigue behavior of implant systems. MATERIAL AND METHODS: The preload and friction coefficient of plasma nitrided abutment screws, as well as settlement of the implant-abutment interface, were measured. Then, the reverse torque values and pullout force were evaluated after cyclic loading. Finally, the fatigue properties of the implant system were investigated with static fracture and dynamic fatigue life tests, and the morphology of the fracture on the surface of the implant system was observed. RESULTS: The plasma nitriding treatment reduced the friction coefficient; increased the preload, settlement value, reverse torque values, pullout force, and static fracture load; and prolonged fatigue life. Furthermore, abutment screws with plasma nitriding treatment showed a different fatigue fracture mode. CONCLUSIONS: Plasma nitriding improved mechanical performance and may be a suitable way to optimize the fatigue behavior of dental implants.

• MeSH
• analýza zatížení zubů metody   MeSH
• design pilíře zubního implantátu MeSH
• podpěry zubní MeSH
• testování materiálů MeSH
• točivý moment MeSH
• tření MeSH
• zubní implantáty * MeSH
• Publikační typ
• časopisecké články MeSH
• Názvy látek
• zubní implantáty * MeSH