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Nafion possesses many interesting properties such as a high ion-conductivity, hydrophilicity, and thermal and chemical stability that make this material highly suitable for many applications including fuel cells and various (bio-)chemical and physical sensors. However, the mechanical properties of a Nafion membrane that are known to be affected by the viscoplastic characteristics of the material itself have a strong impact on the performance of Nafion-based sensors. In this study, the mechanical properties of Nafion under the cyclic loading have been investigated in detail. After cyclic tensile loading (i.e., maximum elongation about 25% at a room temperature and relative humidity about 40%) a time-dependent recovery comes into play. This recovery process is also shown being strain-rate dependent. Our results reveal that the recovery behavior weakens after performing several stress-strain cycles. Present findings can be of a great importance in future design of various chemical and biological microsensors and nanosensors such as hydrogen or glucose ones.
- Klíčová slova
- Nafion, cyclic loading, mechanical properties, mechanical tests, viscoplastic properties,
- Publikační typ
- časopisecké články MeSH
This study is focused on the mechanical properties and service life (safety) evaluation of hybrid adhesive bonds with shaped overlapping geometry (wavy-lap) and 100% natural cotton fabric used as reinforcement under cyclic loading using various intensities. Cyclic loading were implemented between 5-50% (267-2674 N) and 5-70% (267-3743 N) from the maximum strength (5347 N) measured by static tensile test. The adhesive bonds were loaded by 1000 cycles. The test results demonstrated a positive influence of the used reinforcement on the mechanical properties, especially during the cyclic loading. The adhesive bonds Tera-Flat withstood the cyclic load intensity from 5-70% (267-3743 N). The shaped overlapping geometry (wavy-lap bond) did not have any positive influence on the mechanical performance, and only the composite adhesive bonds Erik-WH1 and Tera-WH1 withstood the complete 1000 cycles with cyclic loading values between 5-50% (267-2674 N). The SEM analysis results demonstrated a positive influence on the fabric surface by treatment with 10% NaOH aqueous solution. The unwanted compounds (lignin) were removed. Furthermore, a good wettability has been demonstrated by the bonded matrix material. The SEM analysis also demonstrated micro-cracks formation, with subsequent delamination of the matrix/reinforcement interface caused by cyclic loading. The experimental research was conducted for the analysis of hybrid adhesive bonds using curved/wavy overlapping during both static and cyclic loading.
- Klíčová slova
- SEM, cyclic fatigue, mechanical properties, natural cotton fabric, polymer composite, quasi-static test, safety, service life, wavy-lap bond,
- Publikační typ
- časopisecké články MeSH
Undoubtedly, a better understanding and the further development of approaches for damage tolerant component design of AM parts are among the most significant challenges currently facing the use of these new technologies. This article presents a thorough overview of the workshop discussions. It aims to provide a review of the parameters affecting the damage tolerance of parts produced by additive manufacturing (shortly, AM parts) with special emphasis on the process parameters intrinsic to the AM technologies, the resulting defects and the residual stresses. Based on these aspects, basic concepts are reviewed and critically discussed specifically for AM materials: Criteria for damage tolerant component design;Criteria for the determination of fatigue and fracture properties;Strategies for the determination of the fatigue life in dependence of different manufacturing conditions;Methods for the quantitative characterization of microstructure and defects;Methods for the determination of residual stresses;Effect of the defects and the residual stresses on the fatigue life and behaviour. We see that many of the classic concepts need to be expanded in order to fit with the particular microstructure (grain size and shape, crystal texture) and defect distribution (spatial arrangement, size, shape, amount) present in AM (in particular laser powder bed fusion). For instance, 3D characterization of defects becomes essential, since the defect shapes in AM are diverse and impact the fatigue life in a different way than in the case of conventionally produced components. Such new concepts have immediate consequence on the way one should tackle the determination of the fatigue life of AM parts; for instance, since a classification of defects and a quantification of the tolerable shapes and sizes is still missing, a new strategy must be defined, whereby theoretical calculations (e.g. FEM) allow determining the maximum tolerable defect size, and non-destructive testing (NDT) techniques are required to detect whether such defects are indeed present in the component. Such examples show how component design, damage and failure criteria, and characterization (and/or NDT) become for AM parts fully interlinked. We conclude that the homogenization of these fields represents the current challenge for the engineer and the materials scientist.
- Klíčová slova
- Additive manufacturing, component assessment, damage tolerance, defects, fatigue loading, residual stresses,
- Publikační typ
- časopisecké články MeSH
The research is focused on the evaluation of mechanical properties of adhesive bonds with a composite layer of adhesive to increase their service life (safety) under cyclic loading of different intensities. Cyclic loading represents a frequent cause of adhesive bond failure and, thus, a reduction in their service life. Waste from the production of coconut oil, that is, coconut shells in the form of particles, was used as a filler. Coconut shells are in most cases incinerated or otherwise uselessly incinerated, but they can also be used as a natural filler. Cyclic loading (quasi-static tests) was performed for 1000 cycles in two intensities, that is, 5-30% (157-940 N) of maximum force and 5-50% (157-1567 N) of maximum force. The results of the experiment showed a positive effect of the added filler, especially at an intensity of 5-50%, when the service life of adhesive bonds with a composite adhesive layer (AB10, AB20, AB30) increased compared to adhesive bonds without added AB0 filler, which did not withstand the given intensity. A more pronounced viscoelastic behavior of adhesive bonds was demonstrated at an intensity of 5-50% between the 1st and 1000th cycle. SEM analysis showed reduced wetting of the filler and matrix and delamination due to cyclic loading.
- Klíčová slova
- SEM, coconut shell powder, cracking, material utilization, mechanical properties, natural filler, quasi-static test, secondary product,
- Publikační typ
- časopisecké články MeSH
- MeSH
- AMP cyklický krev MeSH
- dopamin-beta-hydroxylasa krev MeSH
- dospělí MeSH
- kyseliny mastné neesterifikované krev MeSH
- lidé středního věku MeSH
- lidé MeSH
- tělesná námaha * MeSH
- Check Tag
- dospělí MeSH
- lidé středního věku MeSH
- lidé MeSH
- mužské pohlaví MeSH
- ženské pohlaví MeSH
- Publikační typ
- časopisecké články MeSH
- Názvy látek
- AMP cyklický MeSH
- dopamin-beta-hydroxylasa MeSH
- kyseliny mastné neesterifikované MeSH
The evaluation of changes in shear resistance on soft (or weathered) rock joints under cyclic shear loads with constant normal load (CNL) and constant normal stiffness (CNS) significantly contributes to increasing the safety and stability of rock slopes and underground structures. In this study, a series of cyclic shear tests were conducted on simulated soft rock joints with regular (15°-15°, 30°-30°) and irregular (15°-30°) asperities under different normal stiffnesses (kn). The results indicated that the first peak shear stress increases with the increase in kn up to the normal stiffness of the joints (knj). Beyond knj, no significant change was observed in the peak shear stress. The difference in peak shear stress between regular (30°-30°) and irregular joints (15°-30°) increases as kn increases. The minimum difference of peak shear stress between regular and irregular joints was observed (8.2%) under CNL and the maximum difference was found (64.3%) on knj under CNS. The difference in peak shear stress between the first and subsequent cycles significantly increases as both the joint roughness and kn increases. A new shear strength model is developed to predict peak shear stress of the joints for different kn and asperity angles under cyclic shear loads.
- Klíčová slova
- cyclic shear loads, normal stiffness, regular and irregular joints, rock joint roughness, soft rock joints,
- Publikační typ
- časopisecké články MeSH
This paper describes and presents an experimental program of low-cycle fatigue tests of austenitic stainless steel 08Ch18N10T at room temperature. The low-cycle tests include uniaxial and torsional tests for various specimen geometries and for a vast range of strain amplitude. The experimental data was used to validate the proposed cyclic plasticity model for predicting the strain-range dependent behavior of austenitic steels. The proposed model uses a virtual back-stress variable corresponding to a cyclically stable material under strain control. This internal variable is defined by means of a memory surface introduced in the stress space. The linear isotropic hardening rule is also superposed. A modification is presented that enables the cyclic hardening response of 08Ch18N10T to be simulated correctly under torsional loading conditions. A comparison is made between the real experimental results and the numerical simulation results, demonstrating the robustness of the proposed cyclic plasticity model.
- Klíčová slova
- austenitic steel 08Ch18N10T, cyclic hardening, cyclic plasticity, experiments, finite element method, low-cycle fatigue,
- Publikační typ
- časopisecké články MeSH
- MeSH
- AMP cyklický krev MeSH
- dopamin-beta-hydroxylasa krev MeSH
- dospělí MeSH
- katecholaminy krev MeSH
- lidé MeSH
- prostaglandiny A krev MeSH
- prostaglandiny E krev MeSH
- prostaglandiny F krev MeSH
- prostaglandiny krev MeSH
- tělesná námaha * MeSH
- Check Tag
- dospělí MeSH
- lidé MeSH
- mužské pohlaví MeSH
- Publikační typ
- časopisecké články MeSH
- Názvy látek
- AMP cyklický MeSH
- dopamin-beta-hydroxylasa MeSH
- katecholaminy MeSH
- prostaglandiny A MeSH
- prostaglandiny E MeSH
- prostaglandiny F MeSH
- prostaglandiny MeSH
This paper is oriented toward the specific testing of polymer composites and textile PA66 cords used as reinforcement for composites. The aim of the research is to validate the proposed new testing methods for low-cyclic testing of polymer composites and PA66 cords for the characterization of material parameters useful as input data for computational tire simulations. Part of the research is the design of experimental methods for polymer composites and test parameters such as load rate, preload, and other parameters such as strain for the start and stop of cycle steps. The DIN 53835-13 standard is used for the conditions of textile cord during the first five cycles. A cyclic load is carried out at two temperatures of 20 °C and 120 °C. The testing method includes a hold step for 60 s between each loop. The video-extensometer technique is used for testing. The paper evaluated the effect of temperatures on the material properties of PA66 cords. The true stress-strain (elongation) dependences between points for the video-extensometer of the fifth cycle of every cycle loop are the data results from composite tests. The forcestrain dependences between points for the video-extensometer are the data results from tests of the PA66 cord. These dependencies can be used as input material data of textile cords in the computational simulation of tire casings using a custom material model definition. The fourth cycle in every cycle loop of polymer composites can be considered a stable cycle because the change in the maximum true stress between the fourth and fifth cycles is 1.6%. Other results of this research include a relationship between stress and the number of cycle loops as the second-degree polynomial curve for polymer composites and a simple relationship to describe the value of the force at each end of the cycles for a textile cord.
- Klíčová slova
- PA66, composite, cyclic test, relaxation, temperature, tire, true stress,
- Publikační typ
- časopisecké články MeSH
The paper presents the original results of cyclic testing of materials that are identical in chemical composition but produced by two different technologies: conventional metallurgy and additive manufacturing. For the aluminium alloy AlSi10Mg and the austenitic steel 316L, tensile curves, tension-compression and torsion alternating fatigue curves are experimentally obtained and presented. The experimental results are compared for two fabrication technologies-conventional metallurgy and additive DLMS technology. The results indicate a significant effect of anisotropy on the fatigue performance of the AM materials and a different slope of the fatigue life curves in the cyclic torsion versus cyclic tension-compression. The static and, in particular, the fatigue properties of both materials are discussed in relation to the microstructure of the materials after conventional production and after additive manufacturing. This comparison allowed us to explain both the causes of the anisotropy of the AM materials and the different slope of the curves for normal and shear stresses under cyclic loading. Using the example of the strength assessment of bicycle frames, the possibility of progressively wider use of additive manufacturing for load-bearing structures is presented.
- Klíčová slova
- 316L, additive manufacturing, aluminium alloy, fatigue properties, tension and torsion cyclic tests,
- Publikační typ
- časopisecké články MeSH